Pesticide Residue Testing
& MRL Compliance

Accredited multi-residue pesticide residue testing by LC-MS/MS to verify your products meet strict Maximum Residue Limits (MRLs) for the EU, Japan, and US markets.

Accreditation
ISO/IEC 17025:2017 · Cert L24-482-R2
Method
AOAC 2007.01 · LC-MS/MS
Coverage
200+ Pesticides | EU, Japan, USA
Turnaround
5–7 Business Days · Rush 48–72h

Avoid Border Rejections & DWPE

Exporting food products requires navigating a complex web of global pesticide regulations. A product that is compliant in the US may be rejected in the European Union, where limits are significantly stricter. Avoid costly FDA import detention due to MRL violations.

Pesticide residues are a major subset of chemical food contaminants. AGT Food Labs delivers high-sensitivity pesticide residue testing using AOAC 2007.01 (SOP 070) on LC-MS/MS to detect trace levels of polar and semi-polar residues. Each analytical run validates compliance against your destination MRL, helping prevent shipment rejections and protecting your global supply chain.

Common Triggers for Pesticide Residue Testing

Most exporters request analysis when one of these business situations comes up.

📦Pre-Shipment Verification

A new lot of produce, grain, spice, tea, or dried botanical is heading overseas and the importer requires a Certificate of Analysis before the container ships.

🛒Buyer or Retailer Requirement

Major retailers, food service buyers, and private-label brands routinely require third-party multi-residue results as part of their supplier qualification or annual surveillance programs.

🌱Organic Verification

USDA NOP and EU Organic operators screen incoming raw materials and finished lots to defend their organic claim against synthetic pesticide drift, prohibited treatments, or supplier substitution.

⚠️Border Detention or Recall Risk

An FDA DWPE alert, an EU RASFF notification, or a customer complaint has raised contamination concerns. Targeted pesticide residue testing produces the data needed to clear the shipment or scope a corrective action.

🤝New Supplier Onboarding

A new grower, broker, or contract farm is being added to your supply chain and you need a baseline screen to confirm their material meets the same MRLs as your existing approved sources.

📅Annual Surveillance & Due Diligence

Routine surveillance lots — quarterly, semi-annual, or per-harvest — give brand owners documented evidence of "Reasonable Care" if a residue question is later raised by a regulator or customer.

The Pesticide Residue Testing Workflow

Standardized AOAC 2007.01 methodology for accurate, defensible results.

📦
01. Submission
Send 500g of sample for pesticide residue testing. Specify your target export market (e.g., EU, Japan) so we can apply the correct limits.
🧪
02. QuEChERS Prep
We extract residues from the food matrix using the QuEChERS approach (Quick, Easy, Cheap, Effective, Rugged, Safe) per AOAC 2007.01.
🔬
03. LC-MS/MS Analysis
Samples are analyzed by LC-MS/MS per AOAC 2007.01 (SOP 070) under our PJLA ISO/IEC 17025 scope, targeting more than 200 polar and semi-polar pesticides.
📊
04. Compliance Report
A Certificate of Analysis flags any residues that exceed the MRL for your destination market based on the analytical data.

Our Pesticide Residue Testing Services

Tailored screening packages for produce, grain, spice, tea, and botanical exporters.

LC-MS/MS instrument running accredited pesticide residue testing per AOAC 2007.01
Comprehensive

Multi-Residue LC-MS/MS Screen (200+)

Our flagship multi-residue service screens over 200 polar and semi-polar pesticides in a single LC-MS/MS run per AOAC 2007.01 (SOP 070). It supports "Due Diligence" verification across major chemical classes — Organophosphates, Carbamates, Triazoles, Strobilurins, and modern Neonicotinoids.

Complex Matrix Expertise: Unlike many standard labs, we specialize in difficult matrices like spices, tea, dried botanicals, and essential oils. We apply targeted dispersive cleanup steps — PSA (Primary Secondary Amine) and GCB (Graphitized Carbon Black) — to remove pigments and co-extractives that often produce false positives in these high-value products.

Key Chemical Classes:
  • Organophosphates (Chlorpyrifos)
  • Carbamates
  • Triazole Fungicides
  • Strobilurins
  • Neonicotinoids
USDA NOP and EU Organic verification screen for synthetic pesticide residues by LC-MS/MS
USDA NOP / EU Organic

Organic Verification Screening

If you claim "Organic," you must prove it. Our LC-MS/MS multi-residue panel screens for synthetic pesticides prohibited under the USDA National Organic Program (NOP) and EU Organic regulations. Even trace levels of prohibited substances can suspend your organic certification.

We specifically monitor for Piperonyl Butoxide (PBO), a synergist often found in "natural" pyrethrum formulations that is strictly prohibited in organic farming, as part of our standard multi-residue protocol.

Methods & Instruments

State-of-the-art LC-MS/MS achieves the low-level detection limits required by EU and Japan regulators.

AGT Food Labs — PJLA-Accredited Methods for Pesticide Residue Testing (Cert L24-482-R2)
Method Name Reference Instrumentation Typical LOQ
QuEChERS Sample PreparationAOAC 2007.01, SOP 070Sample PrepN/A
Multi-Residue Pesticide ScreenAOAC 2007.01, SOP 070LC-MS/MS0.01 mg/kg (10 ppb)

Why LC-MS/MS Defines Modern Pesticide Residue Testing

Liquid Chromatography coupled with tandem Mass Spectrometry separates analytes by polarity and then identifies them through two independent mass transitions per compound. That dual-confirmation step is what gives the technique the selectivity it needs to operate at the EU default MRL of 0.01 mg/kg without false positives. Because most modern active ingredients — Triazoles, Strobilurins, Neonicotinoids, Carbamates, and many Organophosphates — are polar or semi-polar, they ionize cleanly in LC-MS/MS without the derivatization or volatility limitations of older techniques. Our PJLA-accredited scope under AOAC 2007.01 (SOP 070) is purpose-built around this platform, which keeps every reported result defensible to EU, Japanese, and US regulators.

Industries We Serve

Pesticide residue testing across every food and beverage vertical that exports into MRL-regulated markets.

Fresh produce pesticide residue testing for fruits and vegetables

Fresh Produce

Multi-residue screening for fruits, vegetables, leafy greens, and berries shipping into the EU, Japan, and US markets.

Grain and cereal pesticide residue testing

Grains & Cereals

MRL verification for wheat, rice, corn, oats, and pulses — including organophosphate and storage-fumigant residue checks.

Spices, tea, and dried botanical pesticide residue analysis

Spices, Tea & Botanicals

Difficult-matrix expertise with PSA / GCB cleanup for spices, tea, dried herbs, and high-pigment botanical exports.

Essential oils and herbal supplement pesticide testing

Essential Oils & Supplements

Targeted pesticide screening for essential oils, herbal extracts, and dietary supplement raw materials sold internationally.

Global MRL Compliance

Our pesticide residue testing validates results against the regulatory database of your destination market.

European Union (EU)

The strictest framework in the world. If a pesticide is not explicitly approved, the Default MRL is 0.01 mg/kg. Our LC-MS/MS LOQs are designed to meet this stringent requirement.

Japan Positive List

Japan operates on a Positive List system. Any chemical not on the list defaults to 0.01 ppm. We screen specifically for chemicals commonly monitored by Japanese quarantine.

USA (EPA / FDA)

We verify compliance with EPA Tolerances under 40 CFR Part 180. Products exceeding these tolerances are deemed "adulterated" by the FDA.

Frequently Asked Questions

Common questions about pesticide residues, MRLs, and export limits.

What does "MRL" mean?
MRL stands for Maximum Residue Limit — the highest level of a pesticide residue legally tolerated in food or feed. MRLs vary by country and commodity, and accredited laboratory analysis is how exporters demonstrate compliance.
How much sample is required?
We typically require 500g to 1kg of product to ensure a representative sample. For high-value items like saffron or vanilla, smaller quantities can be accepted on consultation.
How long does the analysis take?
Standard turnaround is 5–7 business days. We also offer an expedited Rush Service (48–72 hours) for urgent shipments to meet vessel or flight cut-off times.
Will my results be accepted by EU customs and Japanese quarantine?
Yes. Our analyses are run under PJLA ISO/IEC 17025:2017 accreditation (Cert L24-482-R2) using AOAC 2007.01 (SOP 070). Reports issued under this scope are recognized internationally through the ILAC mutual recognition arrangement, which is what EU customs, Japanese quarantine officers, and most importer compliance teams look for on a third-party Certificate of Analysis.
Does washing produce remove pesticides?
Washing reduces surface residues, but many pesticides are systemic — absorbed inside the fruit or vegetable. Systemic compounds cannot be washed off and will be detected during the analysis.
Why is the limit often 0.01 mg/kg?
In the EU and Japan, if a pesticide does not have a specific established limit for a crop, it defaults to the "Limit of Determination," typically 0.01 mg/kg. In practice this means "zero tolerance" or "not detected."
Why does AGT use LC-MS/MS for pesticide residue testing?
LC-MS/MS is the workhorse for modern multi-residue analysis — it covers polar and semi-polar pesticides (the majority of currently registered active ingredients) at trace level with excellent selectivity. Our PJLA-accredited scope under AOAC 2007.01 (SOP 070) is built around this platform.

Export with Confidence.

Ensure your products pass global border checks with our accredited pesticide residue testing services.

Request a Pesticide Residue Quote
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