Pesticide Residue Testing
Accredited Compliance for Importers & Exporters

An ISO/IEC 17025:2017 accredited laboratory in Houston, Texas. Our pesticide residue testing measures your product against the Maximum Residue Limits of the market it is actually sold into US EPA tolerance, EU, or Japan Positive List before customs does it for you.

Accredited Laboratory
ISO/IEC 17025:2017 · PJLA #117946 · Houston, TX
Method
AOAC 2007.01 (modified) · SOP 070 · LC-MS/MS
Residue Limits Checked
40 CFR 180 · EU Reg. 396/2005 · Japan Positive List
Turnaround
5–7 Business Days · Rush 48–72h

Pesticide Residue Testing That Prevents Border Rejections, DWPE & RASFF Alerts

A container that clears US EPA tolerances can still be refused at an EU port, because the two systems set limits on completely different bases. The EU harmonises one figure across every member state and drops to a default of 0.01 mg/kg wherever no crop-specific figure exists; the US sets each tolerance crop-by-crop under 40 CFR Part 180. Pass one, fail the other and most exporters only discover the gap after the shipment has sailed.

When a residue breaches the limit for its destination, the cost escalates fast: a detained container accruing demurrage, an FDA Import Alert carrying Detention Without Physical Examination status, an EU RASFF notification circulated to every member state, and a buyer who quietly moves the next order elsewhere. Because residues rarely travel alone, importers usually screen the same lot for heavy metals and aflatoxin and mycotoxin at the same time, and hold the results alongside their wider contaminant and import compliance file.

Not every residue test is about a border, though. Domestic manufacturers, US importers clearing FDA and EPA tolerances, private-label brands, and supplement and botanical companies rely on the same accredited pesticide residue testing for routine QA, supplier verification, and label-claim defence the destination simply decides which limit we report your result against.

AGT Food Labs runs a modified AOAC 2007.01 method (SOP 070) on LC-MS/MS under PJLA ISO/IEC 17025:2017 accreditation, certificate L26-535. Every report states the limit that applies to your destination, the measured concentration, and the reporting limit we achieved the three numbers a customs broker, a retail technologist, or an auditor will ask for.

When You Need Pesticide Residue Testing

Six situations that put a residue certificate on the critical path for importers, exporters, and domestic manufacturers alike.

📦Pre-Shipment Verification

A lot of produce, grain, spice, tea, or dried botanical is booked for export and the importer will not release the letter of credit without a third-party Certificate of Analysis against the destination limits.

🛒Buyer or Retailer Requirement

Major retailers, food-service groups, and private-label brands write residue screening into supplier qualification and annual surveillance. Many specify stricter internal thresholds than the statutory MRL often a fraction of it.

🌱Organic Verification

USDA NOP and EU Organic operators screen incoming raw materials and finished lots to defend the organic claim against spray drift, prohibited treatments, or supplier substitution somewhere upstream.

⚠️Border Detention or Recall Risk

An FDA DWPE listing, a RASFF notification, or a customer complaint has already landed. You need defensible data fast either to release the consignment or to scope the corrective action honestly.

🤝New Supplier Onboarding

A new grower, broker, or contract farm enters the supply chain. A baseline screen establishes whether their material clears the same limits as your approved sources, before volume commitments are made.

📅Annual Surveillance & Due Diligence

Routine lots quarterly, semi-annual, or per harvest build the documented evidence of reasonable care that a regulator or customer will ask for after an incident, not before one.

How Pesticide Residue Testing Works Sample to Certificate

A standardised pesticide residue testing workflow — QuEChERS extraction and LC-MS/MS — reported against your destination limits.

📦
01. Submission
Send 500 g of representative sample and name your destination market. That single detail determines which limit database we report against.
🧪
02. QuEChERS Prep
Residues are extracted with the QuEChERS approach Quick, Easy, Cheap, Effective, Rugged, Safe followed by dispersive cleanup matched to the matrix.
🔬
03. LC-MS/MS Analysis
The extract runs on LC-MS/MS under modified AOAC 2007.01 (SOP 070), within our PJLA ISO/IEC 17025:2017 scope, targeting the polar and semi-polar actives that dominate today's registrations.
📊
04. Compliance Report
You receive a Certificate of Analysis stating each detection, its reporting limit, and a clear pass or fail against the destination MRL.

Our Pesticide Residue Testing Services

Screening packages built for produce, grain, spice, tea, and botanical manufacturers, importers, and exporters.

LC-MS/MS instrument running an accredited pesticide residue screen per AOAC 2007.01 at AGT Food Labs Houston
Comprehensive

Multi-Residue Pesticide Screen by LC-MS/MS

Our flagship pesticide residue panel measures a broad range of polar and semi-polar active ingredients in a single LC-MS/MS run under modified AOAC 2007.01 (SOP 070), covering the chemical classes that dominate current registrations — organophosphates, carbamates, triazole fungicides, strobilurins, and neonicotinoids.

Difficult matrices are the point. Spices, tea, dried botanicals, and essential oils defeat a lot of standard panels: chlorophyll, capsaicinoids, and other co-extractives suppress or enhance ionisation and manufacture false positives. We apply targeted dispersive cleanup with PSA (primary secondary amine) and GCB (graphitised carbon black) to strip pigment and co-extractives before injection, so the number on your certificate reflects the sample rather than the matrix.

Key Chemical Classes:
  • Organophosphates (Chlorpyrifos)
  • Carbamates
  • Triazole Fungicides
  • Strobilurins
  • Neonicotinoids
USDA NOP and EU Organic verification screen for prohibited synthetic residues by LC-MS/MS
USDA NOP / EU Organic

Organic Verification Screening

An organic claim is only as strong as the evidence behind it. Our LC-MS/MS panel screens for the synthetic actives prohibited under the USDA National Organic Program and EU Organic regulation, where a single trace detection can trigger an investigation and suspend certification.

We include Piperonyl Butoxide (PBO) as standard — a synergist frequently formulated into "natural" pyrethrum products, prohibited in organic production, and one of the more common causes of an otherwise unexplained positive on an organic lot.

Methods & Instruments

Reporting limits low enough to satisfy the EU default of 0.01 mg/kg.

AGT Food Labs — PJLA-Accredited Methods, Certificate L26-535 (Houston, TX)
Method Name Reference Instrumentation Typical LOQ
QuEChERS Sample PreparationAOAC 2007.01 (modified), SOP 070Sample PrepN/A
Multi-Residue Pesticide ScreenAOAC 2007.01 (modified), SOP 070LC-MS/MS0.01 mg/kg (10 ppb)

Why LC-MS/MS Is the Reference Platform for Pesticide Residue Testing

Liquid chromatography with tandem mass spectrometry separates analytes by polarity, then confirms each one through two independent mass transitions. That dual confirmation is what allows quantitation at 0.01 mg/kg without the false positives that make a certificate unusable. It also suits the chemistry of the modern portfolio: triazoles, strobilurins, neonicotinoids, carbamates, and most organophosphates are polar or semi-polar, so they ionise cleanly without derivatisation or the volatility constraints of older techniques. Our accredited scope was built around this platform for that reason, and it is why results hold up in front of EU, Japanese, and US reviewers.

Scope note: Our accreditation covers pesticides amenable to LC-MS/MS — the polar and semi-polar actives that make up the majority of today's registered products. GC-amenable legacy classes (organochlorines, pyrethroids, and dithiocarbamates) fall outside this scope, and we coordinate them with partner laboratories whenever a full multi-class panel is required. We would rather tell you that up front than have it surface in an audit.

Industries We Serve

Every vertical that ships food or botanicals into a residue-regulated market.

Fresh produce pesticide residue screening for fruits, vegetables and leafy greens

Fresh Produce

Fruits, vegetables, leafy greens, and berries moving into the EU, Japan, and US markets on short shelf-life clocks.

Grain and cereal pesticide residue verification including storage fumigant residues

Grains & Cereals

Wheat, rice, corn, oats, and pulses — including the post-harvest storage treatments that surface long after the field application.

Spices, tea and dried botanical pesticide residue testing with PSA and GCB cleanup

Spices, Tea & Botanicals

High-pigment matrices where PSA and GCB cleanup separates a real detection from a matrix artefact.

Essential oils and herbal supplement raw material residue screening

Essential Oils & Supplements

Essential oils, herbal extracts, and supplement raw materials, where concentration steps multiply any residue present.

Global MRL Compliance

We report your pesticide residue result against the regulatory database of the market you are shipping to, not a generic panel.

United States — 40 CFR Part 180

EPA sets tolerances crop-by-crop, and the FDA treats any product exceeding one as adulterated under the FD&C Act. Where no US tolerance exists for a crop-active pairing, the effective limit is zero. Codex figures apply only where a country has adopted them.

European Union — Reg. 396/2005

The strictest framework in commercial use. Where no crop-specific limit is published, the default falls to 0.01 mg/kg — effectively zero tolerance. Our reporting limits are set to meet that floor rather than approach it.

Japan — Positive List System

Any active absent from the Positive List defaults to 0.01 ppm. We screen specifically for the actives Japanese quarantine monitors most often on imported produce, tea, and botanicals.

Frequently Asked Questions

Pesticide residue testing, Maximum Residue Limits, export thresholds, and what to do when a result comes back over.

What does "MRL" mean?
MRL stands for Maximum Residue Limit — the highest concentration of a given pesticide residue that a regulator legally tolerates in a specific food or feed commodity. Two things make it harder than it sounds: the figure is set per active ingredient and per commodity, and it differs between markets. The same tea shipment can face three different numbers in the EU, Japan, and the US.
How do I find the MRL that applies to my commodity and destination?
You need three pieces of information: the active ingredient, the commodity as the regulator classifies it, and the destination country. The EU publishes a searchable database under Regulation 396/2005, Japan maintains the Positive List, and the US publishes tolerances in 40 CFR Part 180. Commodity classification is where most exporters slip — "dried herbs" and "leafy vegetables" can carry very different limits, and a processing factor may apply to the dried form. Tell us the destination when you submit and we will apply the correct classification.
Will my results be accepted by EU customs and Japanese quarantine?
Yes. Analyses run under our PJLA ISO/IEC 17025:2017 accreditation (certificate L26-535) using modified AOAC 2007.01 (SOP 070). PJLA is a signatory to the ILAC Mutual Recognition Arrangement, which is the mechanism by which accredited reports issued in one economy are recognised in another — and it is what EU customs, Japanese quarantine officers, and importer compliance teams look for on a third-party Certificate of Analysis. Individual buyers may still specify their own nominated laboratory; worth confirming before you ship.
What happens if a result exceeds the MRL?
Do not ship it. A confirmed exceedance found in your own laboratory is a commercial problem; the same exceedance found at a border becomes a regulatory one, with detention costs, a possible Import Alert listing, and a public RASFF entry that your competitors can read. The practical sequence is to confirm the finding on a re-drawn sample, trace it to a field, lot, or supplier, and decide whether the material can be diverted to a market whose limit it does meet. We can support the confirmatory work and the traceback sampling plan.
Can you test high-pigment spices, tea, and botanicals?
Yes — these are the matrices we are built for. High pigment loads and heavy co-extractives cause ion suppression and enhancement, which is why identical material can produce different answers at different laboratories. We apply targeted QuEChERS cleanup with PSA (primary secondary amine) and GCB (graphitised carbon black) to remove chlorophyll and colour compounds before LC-MS/MS, and use matrix-matched calibration so the quantitation reflects the commodity in front of us.
How do EU limits differ from US EPA tolerances?
The EU harmonises a single figure across all member states and applies a default of 0.01 mg/kg to any active without a crop-specific limit. The US sets tolerances individually, crop by crop, under 40 CFR Part 180, and the FDA deems any over-tolerance product adulterated. The consequence for exporters is direct: a lot that is fully compliant in the US can be refused at an EU border on an active that simply has no European approval. We always report against the destination you specify.
Do you screen for substances prohibited under USDA NOP and EU Organic?
Yes. The LC-MS/MS panel covers the synthetic actives prohibited under the USDA National Organic Program and EU Organic regulation, including Piperonyl Butoxide (PBO), a synergist common in "natural" pyrethrum formulations. Because a single trace detection can suspend a certification, the screen gives you documented evidence to defend the claim at audit — and an early warning if drift or substitution has entered your supply chain.
How fast can you turn a shipment around?
Standard turnaround is 5–7 business days from receipt at our Houston laboratory. Rush service at 48–72 hours is available subject to instrument capacity — the usual reason exporters need it is a container already sitting at a port under detention. Contact us before shipping the sample so we can confirm the slot rather than have your material queue.

Export with Confidence.

Get your lot measured against the limits of the market you are shipping to — by an accredited laboratory in Houston, Texas.

Request a Pesticide Residue Testing Quote
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